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This is not usually a problem for Threshold Substances (at least not now see below for historical injustices relating to Threshold Substances), as an adjustment is made, as set out in Technical Document TD2019DL, in order to avoid the risk of false positives arising from an athletes hydration status

Per-Batch HPLC + Disulfide Bond Verification Because the lipolytic conformation depends on an intact Cys7-Cys14 disulfide bond, every released lot is checked both by HPLC for peptide purity and by non-reducing LC-MS or Ellman's reagent analysis for disulfide bond integrity

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